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Introducing the book “Instrumental Methods of Analysis" is something that fills me with an incredible amount of joy. The content of this book has been meticulously crafted to adhere to the curriculum for Bachelor of Pharmacy students that has been outlined by the Pharmacy Council of India. An effort has been made to investigate the topic using terminology that is as straightforward as possible in order to make it more simply digestible for pupils. The book has a number of illustrations, such as flowcharts and diagrams that make it simple for students to comprehend complex ideas. It is the author's honest desire that both students and academicians would take something helpful away from reading this book. Instrumental Methods of Analysis imparts fundamental knowledge on the principles and instrumentation of some of the most commonly used Hyphenated techniques. This book caters to the need of the students and analysts in various fields for a thorough understanding of the construction of various analytical instruments and their principles. A detailed study of the book will make the readers proficient in spectroscopic and chromatographic techniques that are covered in the book, their applications including limitations.